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The hydrolysis of AlN powder and its use for the synthesys of nanostructured alumina coatings

Author(s): Andraž Kocjan (Author), Tomaž Kosmač (Supervisor), Kristoffer Krnel (Co-Supervisor)

Year: 2010

Type: Doctoral dissertation

he thesis describes a study of aluminum nitride (AlN) powder hydrolysis in the temperature range between 5 °C and 90 °C. The analysis of the temperature dependence of the course of the hydrolysis and the reaction kinetics, along with a mechanistic model set up for the hydrolysis reactions, gives a …

Solution synthesis of nanoparticles in multicomponent oxide systems

Author(s): Elena-Daniela Ion (Author), Barbara Malič (Supervisor), Iztok Arčon (Co-Supervisor)

Year: 2008

Type: Doctoral dissertation

The study of PbZrO3 (PZ), PbTiO3 (PT) and La2Zr2O7 (LZ) prepared by alkoxide sol-gel synthesis is described. PZ and PT sols were prepared from lead acetate, zirconium and titanium n-butoxide, in n-butanol and hydrolysed with Rw (molar ratio of water per lead acetate) between 2 and 15 in neutral medium …